SYNTHESIS OF ZIRCONIA NANOPARTICLES VIA THERMAL DECOMPOSITION OF ZIRCONIUM COMPLEX WITH CITRIC ACID

Authors

  • Igor V Krivtsov South Ural State University, Chelyabinsk, Russian Federation
  • Anna V Ustimenko South Ural State University, Chelyabinsk, Russian Federation
  • Marina V Il'kaeva South Ural State University, Chelyabinsk, Russian Federation
  • Vyacheslav V Avdin South Ural State University, Chelyabinsk, Russian Federation

Keywords:

ZrO2, zirconia nanoparticles, stability of tetragonal ZrO2

Abstract

The influence of pH value of zirconium oxycitrate solution on formation of ZrO2 nanoparticles prepared via its thermal decomposition has been investigated. Powder X-ray diffractional analysis and transmission electron microscopy have been applied to characterize nanomaterial’s properties. It has been established that the low pH value (pH 2,0) favors formation of non-agglomerated nanoparticles of the mainly tetragonal ZrO2.

Author Biographies

Igor V Krivtsov, South Ural State University, Chelyabinsk, Russian Federation

кандидат химических наук, научный сотрудник научно-образовательного центра «Нанотехнологии»

Anna V Ustimenko, South Ural State University, Chelyabinsk, Russian Federation

магистрант, кафедра экологии и природопользования

Marina V Il'kaeva, South Ural State University, Chelyabinsk, Russian Federation

аспирант, кафедра экологии и природопользования

Vyacheslav V Avdin, South Ural State University, Chelyabinsk, Russian Federation

доктор химических наук, профессор, декан химического факультета

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Surfactant-Induced Nonhydrolytic Synthesis of Phase-Pure ZrO2 Nanoparticles from Metal- Organic and Oxocluster Precursors // M.A. Sliem, D.A. Schmidt, A. Bétard et al. // Chem. Mater. – 2013. –dx.doi.org/10.1021/cm301128a

Published

2013-10-28

Issue

Section

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