Synthesis and Structure of the Adduct Tri(para-tolyl)antimony Dichloride with Cloro(4-nitrophenoxy)tri(para-tolyl)antimony p-Tol<sub>3</sub>SbCl<sub>2</sub>-p-Tol<sub>3</sub>Sb(Cl)OC<sub>6</sub>H<sub>4</sub>(NO<sub>2</sub>-4)
DOI:
https://doi.org/10.14529/chem170107Keywords:
tri(para-tolyl)antimony dichloride, bis(4-nitrophenoxy)tri(para-tolyl)antimony, adduct p-Tol3SbCl2-p-Tol3Sb(Cl)OC6H4(NO2-4), X-ray diffraction analysisAbstract
Chloro(4-nitrophenoxy)tri(para-tolyl)antimony has been synthesized by the interaction of tri(para-tolyl)antimony dichloride with bis(4-nitrophenoxy)tri(para-tolyl)antimony (3:1 mol.) in toluene. The addition compound has been crystallized from the solution as the adduct p-Tol3SbCl2×p-Tol3Sb(Cl)OC6H4(NO2-4). The structure of the adduct has been established by the X-ray diffractionanalysis.References
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