Synthesis and Structure of Tetraphenylantimony β-Isatoximate
Аннотация
(β-Isatoximato)tetraphenylantimony (1) was obtained by the reaction of pentaphenylantimony with β-isatoxime. X-ray diffraction analysis showed that the antimony atom in complex 1 had distorted trigonal-bipyramidal coordination.
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Schmidbaur H., Mitschke K.H. Hydrogendicarboxylat-Ionen als Wasserstoffbrückenverknüpfte Chelatsysteme in Organoantimonverbindungen. Angew. Chem., 1971, vol. 83, no. 4, pp. 149–150. DOI: 10.1002/ange.19710830414.
Sharutin V.V., Senchurin V.S., Sharutina O.K., Panova L.P. Adducts of Tetraphenylstibium Nitrate with Nitric Acid and of Tetraphenylstibium Acetate with Acetic Acid: Syntheses and Structures. Rus. J. Inorg. Chem., 2008, vol. 53, no. 7, pp. 1110–1114. DOI: 10.1134/S0036023608070206.
Sharutin V.V., Sharutina O.K., Bondar’ E.A., Subacheva O.V., Pakusina A.P., Gerasimenko A.V., Sergienko S.S. Synthesis and Structure of (4-Acetyl-3-hydroxyphenoxy)tetraphenylantimony. Rus. J. Gen. Chem., 2003, vol. 73, no. 3, pp. 350–353. DOI: 10.1023/A:1024993400389.
Sharutin V.V., Pakusina A.P., Egorova I.V., Platonova T.P., Gerasimenko A.V., Gerasimenko E.A., Zakharov L.N., Fukin G.K. Synthesis and Structure of Tetraphenylstibonium and Tetraphenylphosphonium Hydrogen Sulfates. Rus. J. Gen. Chem., 2003, vol. 73, no. 4, pp. 536–540. DOI: 10.1023/A:1025676100508.
Sharutin V.V., Sharutina O.K., Pakusina A.P., Platonova T.P., Gerasimenko A.V., Bukvetskii B.V., Pushilin M.A. Synthesis and Structure of Tetra- and Triphenylantimony Organosulfonates. Rus. J. Coord. Chem., 2004, vol. 30, no. 1, pp. 13–22. DOI: 10.1023/B:RUCO.0000011636.28262.d3.
Sharutin V.V., Sharutina O.K., Senchurin V.S. Tetraphenylantimony Aroxides Ph4SbOAr (Ar = C6H4C6H7, C6H2(Br2-2,6)(tert-Bu-4), C6H3(NO2)2-2,4, C6H2(Br2-2,6)(NO2-4)): Synthesis and Structure. Rus. J. Inorg. Chem., 2017, vol. 62, no. 3, pp. 295–300. DOI: 10.1134/S0036023617030147.
Sharutin V.V., Sharutina O.K., Molokova O.V., Pakusina A.P., Gerasimenko A.V., Sergienko A.S., Bukvetskii B.V., Popov D.Yu. Synthesis and Structures of Tetra-and Triarylantimony Oximates. Rus. J. Coord. Chem., 2002, vol. 28, no. 8, pp. 544–553. DOI: 10.1023/A:1019701511840.
Sharutin V.V., Molokova O.V., Sharutina O.K., Akimova T.I., Gerasimenko A.V., Pushilin M.A. Synthesis and Structure of Tetraphenylantimony Oximates Ph4SbON=CRR′(CRR′ = C6H9−C6H9 –2 and R = Ph, R′ = C(O)Ph). Rus. J. Coord. Chem., 2004, vol. 30, no. 8, pp. 559–565. DOI: 10.1023/B:RUCO.0000037435.99654.0a.
Sharutin V.V., Sharutina O.K., Molokova O.V. Synthesis and Structure of Tetra- and Triphenylantimony Salicylaldoximates. Rus. J. Inorg. Chem., 2012, vol. 57, no. 6, pp. 832–837. DOI: 10.1134/S0036023612010226.
Sharutin V.V., Sharutina O.K. Syntheses and Structures of Tetraphenylantimony Oximates: Ph4SbON=CHR (R=C6H4Br–2, C6H4NO2-2, C4H3S). Rus. J. Coord. Chem., 2017, vol. 43, no. 4, pp. 232–237. DOI: 10.1134/S1070328417040054.
Wang G.-C., Xiao J., Yu L., Li J.-Sh., Cui J.-R., Wang R.-Q., Ran F.-X. Synthesis, Crystal Structures and in vitro Antitumor Activities of Some Arylantimony Derivatives of Analogues of Demethylcantharimide. J. Organomet. Chem., 2004, vol. 689, no. 9, pp. 1631–1638. DOI: 10.1016/j.jorganchem.2004.02.015.
Wang G.-C., Lu Y.-N., Xiao J., Yu L., Song H.-B., Li J.-Sh., Cui J.-R., Wang R.-Q., Ran F.-X. Synthesis, Crystal Structures and in vitro Antitumor Activities of Some Organoantimony Arylhydroxamates.
J. Organomet. Chem., 2005, vol. 690, no. 1, pp. 151–156. DOI: 10.1016/j.jorganchem.2004.09.002.
Sharutin V.V., Sharutina O.K., Molokova O.V., Ettenko E.N., Krivolapov D.B., Gubaidullin A.T., Litvinov I.A. Synthesis and Structure of Tetra- and Triarylantimony Oximates. Rus. J. Gen. Chem., 2001, vol. 71, no. 8, pp. 1243–1247. DOI: 10.1023/A:1013220911661.
Bruker (2000) SMART. Bruker Molecular Analysis Research Tool, Versions 5.625 Bruker AXS, Madison, Wisconsin, USA.
Bruker (2000) SAINT Plus Data Reduction and Correction Program Versions 6.02a, Bruker AXS, Madison, Wisconsin, USA.
Doak G.O., Long G.G., Freedman L.D. The Infrared Spectra of Some Phenylsubstituted Pentavalent Antimony Compounds. J. Organomet. Chem., 1965, vol. 4, no. 1, pp. 82–91.
Batsanov S.S. [Atomic Radiuses of the Elements]. Rus. J. Inorg. Chem., 1991, vol. 36, no. 12, pp. 3015–3037. (in Russ.)
Kopf J., Vetter G., Klar G. Nitrosolate und Nitrosolatokomplexe. III. Darstellung und Struktur von Nitrosolsäurederivaten Organosubstituierter Antimon (V)‐, Tellur (IV)‐und Jod (III)‐Verbindungen. Ztschr. Anorg. und Allg. Chem., 1974, vol. 409, no. 3, pp. 285–298. DOI: 10.1002/zaac.19744090304.
Domasevich K.V., Skopenko V.V., Kempe R., Mohir A.A., Siler I., Hojer Je. [Synthesis, Crystal and Molecular structure of Tetraphenylantimony Complex (V) with 2-Isonitroso-2-(4-methylthiazolyl-2)-acetamide]. Rus. J. Inorg. Chem., 1998, vol. 43, no. 2, pp. 246–249. (in Russ.)
Domasevitch K.V., Gerasimchuk N.N., Mokhir A. Organoantimony (V) Cyanoximates: Synthesis, Spectra and Crystal Structures. Inorg. Chem., 2000, vol. 39, no. 6, pp. 1227–1237. DOI: 10.1021/ic9906048.
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